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madmoney69

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1. Add the following Successively into the reaction bottle:
1kg of adb main material,
3L of DMF, (CAS 68-12-2)
850g of anhydrous potassium carbonate, (CAS584-08-7)
680g of bromobutane (CAS 109-65-9)
2. Raise the temperature of the reaction flask to 70-80°C for 5 hours.
3. After the reaction, the solution ① is obtained, and it is cooled to room temperature.
4. Prepare the bucket in advance, add 15L of water,
5. Pour the solution ① into the bucket and cool to room temperature
6. Filter the solid, and then repeatedly wash with water several times until the solution is neutral (pH
test paper can be used to test the pH of the solution),
7. Dry the neutral solution. you will get adb b.
 

DavidDavison2021

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This new product is a real game changer it’s very easy to synthesise and can be easily done in a home environment and believe me I am no chemist and Even I was able to do this, personally after having the process trialed and tested I think this is the only way to survive, plus it’s good product it’s not like the new replacement BS, this is working very well with my line of work. Honestly if I can do it anyone in this forum can, much more easier than I thought. there’s only a few more instructions that the vendors don’t mention which bring the potency very high just like the old stuff, drop me a message I can help you with the extra techniques to make it strong like the old stuff
Basil587I seen this a couple months back, I didnt think is was legit after asking a buddy who runs a lab.
 

Jailhmp

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Who can assist me with this with some videos showing the process
JailhmpI will
1. Add the following Successively into the reaction bottle:
1kg of adb main material,
3L of DMF, (CAS 68-12-2)
850g of anhydrous potassium carbonate, (CAS584-08-7)
680g of bromobutane (CAS 109-65-9)
2. Raise the temperature of the reaction flask to 70-80°C for 5 hours.
3. After the reaction, the solution ① is obtained, and it is cooled to room temperature.
4. Prepare the bucket in advance, add 15L of water,
5. Pour the solution ① into the bucket and cool to room temperature
6. Filter the solid, and then repeatedly wash with water several times until the solution is neutral (pH
test paper can be used to test the pH of the solution),
7. Dry the neutral solution. you will get adb b.
is there any videos for this please
 

orgasmatron

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Does anyone know if the reaction needs cooling at any point or is only heating necessary?
Can DMA ( N,N-dimethylacetamide )be used instead of DMF?
Is product loss during water washes a concern?

1. Add the following Successively into the reaction bottle:
1kg of adb main material,
3L of DMF, (CAS 68-12-2)
850g of anhydrous potassium carbonate, (CAS584-08-7)
680g of bromobutane (CAS 109-65-9)
2. Raise the temperature of the reaction flask to 70-80°C for 5 hours.
3. After the reaction, the solution ① is obtained, and it is cooled to room temperature.
4. Prepare the bucket in advance, add 15L of water,
5. Pour the solution ① into the bucket and cool to room temperature
6. Filter the solid, and then repeatedly wash with water several times until the solution is neutral (pH
test paper can be used to test the pH of the solution),
7. Dry the neutral solution. you will get adb b.
madmoney69
 

BackstagePanther

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What is this ADB material? We can find a precursor (2S)-2-[(5-bromo-1-butyl-1H-indazol-3-yl)formamido]-3,3-dimethylbutanamide
is this procedure described here going to work with that precursor?
 

WillD

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What is this ADB material? We can find a precursor (2S)-2-[(5-bromo-1-butyl-1H-indazol-3-yl)formamido]-3,3-dimethylbutanamide
is this procedure described here going to work with that precursor?
BackstagePantherYou are talking about the end substance, not a precursor
 
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