4MMC/MEC large crystals

[Chemix-Express]

Well-cleaned powder, low dissolving temp and this is what it looks like after standing motionless at room temperature for 18h

 

[$!$]

Well-cleaned powder, low dissolving temp and this is what it looks like after standing motionless at room temperature for 18h

Chemix-ExpressNow i know your way is fuking easy haha....
2 weeks i try and i found your trick xD good job and thanks for share video bro

 

[HerrHaber]

X-ray diffraction pattern would make this more convincing (haven't seen such 4MMC since 2010, therefore I know they can be as such but I never personally obtained them). P.S. I haven't got any actual competence in interpreting XRD data...

 

[Gordon Ramsay]

Acidified into the aeq. layer, cleaned the aeq. layer with DCM and crystallized with 2:1 Water:Acetone solution

 

[$!$]

Acidified into the aeq. layer, cleaned the aeq. layer with DCM and crystallized with 2:1 Water:Acetone solution

View attachment 34788

Gordon Ramsayhow much days u made bro ??
I made similar in 1 day tomorrow i show u form 50g how my looks

 

[Gordon Ramsay]

how much days u made bro ??
I made similar in 1 day tomorrow i show u form 50g how my looks

$!$I evaporate at RT, a few days

What technique do you do to yield this in one day? Gradual cooling in the freezer?

 

[$!$]

24h